反应 #2267054
ord-641d855038954af3b7002d2a416610d7
反应方程式
p-toluenesulphonic acid monohydrate
resorcinol
→
p-Toluenesulphonic Acid
反应条件
详细条件
See reaction.notes.procedure_details.
后处理
- 1其他An antireflective composition was prepared
- 2workup.DISSOLUTIONAfter dissolution
- 3过滤the solution was filtered through a polypropylene
- 4过滤filter with a 0.2 um pore size
实验过程
An antireflective composition was prepared by dissolving together 0.6682 g of the polymer of Example 1, 0.1177 g of the trimeric condensate of resorcinol and diethylol-p-cresol (plasticizer), 0.0990 g of Powderlink 1174 crosslinker (from Cytec Industries), an acid crosslinking catalyst consisting of 0.009 g of p-toluenesulphonic acid monohydrate (Aldrich), 0.0072 g of FC 430 surfactant (3M Corp.) and 30.96 g of proylene glycol methyl ether alcohol solvent. After dissolution, the solution was filtered through a polypropylene filter with a 0.2 um pore size.