反应 #2223

反应方程式

p-chlorobenzoic hydrazide

chloroacetyl chloride

→

N'-chloroacetyl-4-chlorobenzoic hydrazide

溶剂

dioxane

反应条件

后处理

1. 1
   温度The resulting mixture was refluxed for three hours
2. 2
   过滤filtered
3. 3
   洗涤The resulting solid was washed with ethyl ether
4. 4
   其他dried

实验过程

To a solution of p-chlorobenzoic hydrazide (11.2 g) in dioxane (100 ml) was added chloroacetyl chloride (6 ml). The resulting mixture was refluxed for three hours, cooled to room temperature and filtered. The resulting solid was washed with ethyl ether and dried to yield N'-chloroacetyl-4-chlorobenzoic hydrazide as white solid.

来源