反应 #2200579

ord-1c63baaa7b784e589ea1319894e1fcf4

反应方程式

CCOC(=O)CC(O)CCl
ethyl 4-chloro-3-hydroxybutyrate
C[Si](C)Cl
DMCS
CCOC(=O)CC(=O)CCl
Ethyl 4-Chloroacetoacetate

反应条件

详细条件
See reaction.notes.procedure_details.

后处理

  1. 1
    其他was carried out at 150° C

实验过程

The quantitation of ethyl 4-chloro-3-hydroxybutyrate was carried out by gas chromatography. Thus, using a glass column (ID 3 mm×1 m) packed with PEG-20M Chromosorb WAW DMCS 10%, 80/100 mesh (product of GL Sciences Inc.), chromatography was carried out at 150° C. The detection was made by FID.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US07432095B2uspto-grants-2008_10