反应 #2195502

反应方程式

product

9-Benzyl-7,7,11,11-tetrafluoro-1,5-dithia-9-azaspiro[5.5]undecane

→

title compound

1-Benzyl-3,3,5,5-tetrafluoropiperidine

反应条件

后处理

1. 1
   其他purify by silica gel chromatography

实验过程

React 4.0 mmol of the product of Example 29 with Raney nickel according to the general procedure set forth in Example 23 and purify by silica gel chromatography using methylene chloride/methanol/saturated NH4OH as eluant to yield the title compound.

来源