反应 #2195501

反应方程式

product

9-Benzyl-7,7,11,11-tetrafluoro-1,5-dithia-9-azaspiro[5.5]undecane-8,10-dione

lithium aluminum hydride

→

title compound

9-Benzyl-7,7,11,11-tetrafluoro-1,5-dithia-9-azaspiro[5.5]undecane

反应条件

后处理

1. 1
   其他Purify by silica gel chromatography

实验过程

React 4.9 mmol of the product of Example 21 with lithium aluminum hydride, using the general procedure set forth in Example 1. Purify by silica gel chromatography using methylene chloride/methanol/saturated NH4OH as eluant to yield the title compound.

来源