反应 #2183328

ord-7301675b1dca416f89ab69e62edac470

反应方程式

CCOc1ccc(Br)cn1
5-bromo-ethoxy-pyridine
O=C1CCC2(CC1)OCCO2
1,4-dioxa-spiro[4.5]decan-8-one
CCOc1ccc(C2(O)CCC3(CC2)OCCO3)cn1
title compound
CCOc1ccc(C2(O)CCC3(CC2)OCCO3)cn1
8-(6-Ethoxy-pyridin-3-yl)-1,4-dioxa-spiro[4.5]decan-8-ol

溶剂

反应条件

详细条件
See reaction.notes.procedure_details.

实验过程

The title compound was prepared as a white solid from 5-bromo-ethoxy-pyridine (Aldrich) and 1,4-dioxa-spiro[4.5]decan-8-one in ether using the procedure described in Step A of Example 1.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US08450304B2uspto-grants-2013_05