反应 #216927

ord-756a9c803026480d97beaf6f8835d04d

反应方程式

Fc1ccc2c(c1)Cc1ccccc1[C@H]1CNCCN21
(14bS)-8-fluoro-1,2,3,4,10,14b-hexahydrodibenzo[c,f]pyrazino[1,2-a]azepine
O=C1c2ccccc2C(=O)N1CCBr
N-(2-bromoethyl)phthalimide
O=C1c2ccccc2C(=O)N1CCN1CCN2c3ccc(F)cc3Cc3ccccc3[C@H]2C1
title compound
收率 91.0%
O=C1c2ccccc2C(=O)N1CCN1CCN2c3ccc(F)cc3Cc3ccccc3[C@H]2C1
(14bS)-2-(2-Phthalimidoethyl)-8-fluoro-1,2,3,4,10,14b-hexahydrodibenzo[c,f]pyrazino[1,2-a]azepine
收率 91.0%

反应条件

详细条件
See reaction.notes.procedure_details.

实验过程

Following a procedure similar to that described in Preparation 14(a), but using (14bS)-8-fluoro-1,2,3,4,10,14b-hexahydrodibenzo[c,f]pyrazino[1,2-a]azepine and N-(2-bromoethyl)phthalimide, the title compound was obtained in a yield of 91%.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US05470851uspto-grants-1995_11