反应 #216214

ord-1d1526befd3a4af7a497eab7cf9d512e

反应方程式

CC(C)=CCCC(C)=CCCC(C)=CCO
farnesol
O=C(Cl)Cc1ccccc1
phenylacetyl chloride
→
CC(C)=CCCC(C)=CCCC(C)=CCOC(=O)Cc1ccccc1
oil
收率 54.0%
CC(C)=CCCC(C)=CCCC(C)=CCOC(=O)Cc1ccccc1
FARNESYL PHENYLACETATE
收率 54.0%

反应物

CC(C)=CCCC(C)=CCCC(C)=CCO
farnesol
O=C(Cl)Cc1ccccc1
phenylacetyl chloride

试剂

无

反应条件

详细条件
See reaction.notes.procedure_details.

后处理

  1. 1
    温度was refluxed for 2.5 hours
  2. 2
    萃取Extraction
  3. 3
    其他with hexane, and purification

实验过程

A mixture of farnesol (440 mg, 2 mmol) and phenylacetyl chloride (584 mg, 7.8 mmol) was refluxed for 2.5 hours. Extraction with hexane, and purification yielded 368 mg (yield: 54%) of oil having the following physical properties.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US05466718uspto-grants-1995_11