反应 #216213

ord-62198d5ca2b64db4ba0d8e928998ba71

反应方程式

CC(C)=CCCC(C)=CCCC(C)=CCO
farnesol
CC(C)C(=O)Cl
isobutyryl chloride
→
CC(C)=CCCC(C)=CCCC(C)=CCOC(=O)C(C)C
oil
收率 7.8%
CC(C)=CCCC(C)=CCCC(C)=CCOC(=O)C(C)C
FARNESYL ISOBUTYRATE
收率 7.8%

反应物

CC(C)=CCCC(C)=CCCC(C)=CCO
farnesol
CC(C)C(=O)Cl
isobutyryl chloride

试剂

无

反应条件

详细条件
See reaction.notes.procedure_details.

后处理

  1. 1
    温度was refluxed for 2 hours
  2. 2
    萃取Extraction
  3. 3
    其他with hexane, and purification

实验过程

A mixture of farnesol (356 mg, 1.6 mmol) and isobutyryl chloride (407 mg, 3.8 mmol) was refluxed for 2 hours. Extraction with hexane, and purification yielded 35.9 mg (yield: 7.8%) of oil having the following physical properties.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US05466718uspto-grants-1995_11