反应 #2139926

ord-30ba1818977d4670a24a24a0170e33ea

反应方程式

C=COCC
Ethyl vinyl ether
OCc1ccccc1
benzyl alcohol
C=COCc1ccccc1
benzyl vinyl ether

反应条件

详细条件
See reaction.notes.procedure_details.

后处理

  1. 1
    萃取The reaction mixture was extracted with ethyl acetate
  2. 2
    萃取the ethyl acetate extract
  3. 3
    洗涤was washed with water
  4. 4
    workup.DISTILLATIONfollowed by distillation in vacuo

实验过程

Ethyl vinyl ether was mixed in benzyl alcohol, to which was then added mercury acetate, and the mixture was stirred at room temperature for 12 hours. The reaction mixture was extracted with ethyl acetate and the ethyl acetate extract was washed with water, followed by distillation in vacuo to obtain benzyl vinyl ether.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US07326513B2uspto-grants-2008_02