反应 #2134

ord-e9220e2450c24e59bc6ac895e81aca07

反应方程式

CCOP(=O)(CCCCCn1c(=O)c2[nH]cnc2n(C)c1=O)OCC
diethyl [5-(3-methyl-xanthin-1-yl)pentyl]phosphonate
CCCCBr
1-bromobutane
→
CCCCn1cnc2c1c(=O)n(CCCCCP(=O)(OCC)OCC)c(=O)n2C
Diethyl [5-(7-butyl-3-methylxanthin-1-yl)pentyl]phosphonate

反应物

CCOP(=O)(CCCCCn1c(=O)c2[nH]cnc2n(C)c1=O)OCC
diethyl [5-(3-methyl-xanthin-1-yl)pentyl]phosphonate
CCCCBr
1-bromobutane

试剂

无

反应条件

详细条件
See reaction.notes.procedure_details.

实验过程

The title substance was prepared from 0.008 mol of diethyl [5-(3-methyl-xanthin-1-yl)pentyl]phosphonate and 0.01 mol of 1-bromobutane analogously to Example 46.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US05728686uspto-grants-1998_03