反应 #2063057

反应方程式

chlorobenzene

sodium carbonate

styrene

propylene carbonate

→

stilbene

溶剂

diethyl ether

反应条件

后处理

1. 1
   workup.ADDITIONis added
2. 2
   过滤the mixture is filtered

实验过程

Under argon, a solution containing 122 mg of chlorobenzene, 106 mg of sodium carbonate, 157 mg of styrene and 1 ml of propylene carbonate stabilized 0.001 M colloid solution is heated at 155° C. with stirring in a sealed vessel for 17 h. At the end of the reaction, 2 ml of diethyl ether is added, and the mixture is filtered. The yield of isolated trans-stilbene is 15%.

来源