反应 #2045077

反应方程式

dibenzo[b,d]thiophene

n-butyllithium

hexane

→

dibenzo[b,d]thiophen-4-yl lithium

溶剂

ether

反应条件

后处理

1. 1
   温度heated at 35° C. oil bath for 2 h

实验过程

Into a solution of dibenzo[b,d]thiophene (4.80 g, 26.1 mmol) in ether (70 mL) was added n-butyllithium solution in hexane (2.5 M, 9.48 mL, 23.70 mmol) dropwise at −78° C., and the solution was allowed to warm to room temperature and then heated at 35° C. oil bath for 2 h to yield a red solution of dibenzo[b,d]thiophen-4-yl lithium.

来源