反应 #2021473

反应方程式

perfluorooctanesulfonic acid

silver carbonate

→

silver perfluorooctanesulfonate

溶剂

water

反应条件

后处理

1. 1
   workup.ADDITIONwas added
2. 2
   workup.STIRRINGAfter stirring at room temperature for 3 days
3. 3
   过滤the mixture was filtered
4. 4
   过滤the obtained filter-cake
5. 5
   洗涤was washed with 10 parts of ion-exchange water
6. 6
   干燥20 parts of diethylether and dried

实验过程

Into a four-necked flask were charged 75 parts of perfluorooctanesulfonic acid and 100 parts of water, and 21.4 parts of silver carbonate was added thereto with stirring. After stirring at room temperature for 3 days, the mixture was filtered and the obtained filter-cake was washed with 10 parts of ion-exchange water, then 20 parts of diethylether and dried to give 60.3 parts of silver perfluorooctanesulfonate.

来源