反应 #2006428

ord-716a36f0ef684f5a928e9f76541cd645

反应方程式

O=[Si]([O-])[O-].[Na+].[Na+]
sodium water glass
O
water
[Na+].[Na+].[Na+].[Na+].[O-][Si]([O-])([O-])[O-]
sodium silicate

试剂

反应条件

详细条件
See reaction.notes.procedure_details.

实验过程

300 ml of sodium water glass was mixed with 2700 ml of de-ionized water to form an aqueous solution of sodium silicate, which was passed through a cationic exchange resin column, thereby forming silicic acid. 5 wt % aqueous KOH was added gradually at a temperature below 80° C. (preferably, 70-80° C.) until the pH value of the aqueous solution was greater than 10 so that the silicic acid was alkalized and under went polycondensation. The reaction product was cooled to 40° C., and was added with 300 ml of 10 wt % sodium aluminate aqueous solution. After 40 minutes, the reaction product was passed through a cationic exchange resin column to obtain a clear silica sol A.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US08167684B2uspto-grants-2012_05