反应 #1973963

反应方程式

3,4-dinitroaniline

methanesulfonyl chloride

pyridine

→

title compound

N-(3,4-dinitrophenyl)methanesulfonamide

溶剂

CH2Cl2

反应条件

后处理

1. 1
   浓缩Mixture was concentrated under vacuum

实验过程

A mixture of 3,4-dinitroaniline (5.27 g, 28.8 mmol), methanesulfonyl chloride (3.36 mL, 43.1 mmol) and pyridine (5.82 mL, 71.9 mmol) in CH2Cl2 (100 mL) was stirred for 24 h. Mixture was concentrated under vacuum to provide a crude semi-solid title compound that was used without further purification.

来源