反应 #1880950
ord-503e25d5855441cebc99cb4ab3010d46
反应方程式
butadiene
orthoxylene
→
5-orthotolyl pentene
反应条件
详细条件
See reaction.notes.procedure_details.
后处理
- 1其他The synthesis of 2,6-NDC typically includes several steps
实验过程
The synthesis of 2,6-NDC typically includes several steps. In a typical synthesis, orthoxylene and butadiene are reacted over an alkali metal or other catalyst to yield a 5-orthotolyl pentene (5-OTP) alkenylation product. The 5-OTP is then cyclized over an acid catalyst to yield 1,5 dimethyltetralin (1,5-DMT). The 1,5 DMT is dehydrogenated over a noble metal or other dehydrogenation catalyst to yield 1,5 dimethylnaphthalene (1,5-DMN), which is subsequently isomerized to produce 2,6-DMN.