反应 #1880949

ord-e3da1ad9914a4f978033cb83e4daf5c9

反应方程式

OCCC1CCCCC1
Cyclohexylethyl alcohol
C=COCC
ethyl vinyl ether
C=COCCC1CCCCC1
cyclohexylethyl vinyl ether

反应条件

详细条件
See reaction.notes.procedure_details.

后处理

  1. 1
    其他The resultant reaction mixture
  2. 2
    萃取was extracted with ethyl acetate and water
  3. 3
    洗涤the extract was washed with water
  4. 4
    workup.DISTILLATIONdistilled under reduced pressure

实验过程

Cyclohexylethyl alcohol was mixed with ethyl vinyl ether. Mercury acetate was added thereto and this mixture was stirred at room temperature for 12 hours. The resultant reaction mixture was extracted with ethyl acetate and water, and the extract was washed with water and then distilled under reduced pressure to obtain cyclohexylethyl vinyl ether (X-1) as the target compound.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US07022456B2uspto-grants-2006_04