反应 #1824338

反应方程式

pyrrolidine

lawsone

THF

p-toluenesulphonic acid

lawsone

→

title compound

2-(5,5-dimethylhex-1-enyl)-3-hydroxy-naphthalene-1,4-dione

溶剂

benzene

反应条件

实验过程

The aldehyde (8.46 mmol) was coupled to lawsone following the procedure set out in Example 42 using lawsone (1.18 g),THF (20 ml), pyrrolidine (672 μl), benzene (40 ml) and p-toluenesulphonic acid (1.95 g). 391 mg of the title compound was isolated after purification.

来源