反应 #1824310

ord-9f25ba1a487943059b248d1ea9d2e6a2

反应方程式

O=C([O-])CN(CCN(CC(=O)[O-])CC(=O)O)CC(=O)O.[Na+].[Na+]
disodium EDTA dihydrate
O=C([O-])[O-].[Na+].[Na+]
sodium carbonate
O=C(O)CN(CCN(CC(=O)O)CC(=O)O)CC(=O)O
Disodium EDTA

反应条件

详细条件
See reaction.notes.procedure_details.

后处理

  1. 1
    其他is provided in line 320
  2. 2
    workup.ADDITIONThe resulting solution is then mixed within a tubular reactor 316

实验过程

A seasoned Kodak 885 hardened fixer was treated in the silver recovery unit 300 shown in FIG. 3, which incorporates a silver precipitating unit 80 according to U.S. Pat. No. 5,437,492 and described above. A continuous stream of untreated Kodak 855 hardened fixer at a flow rate of 100 mls/minute is provided in line 320. A solution of 7.5 g/l disodium EDTA dihydrate and 35 g/l sodium carbonate in storage vessel 310 is drawn off via line 311 by pump 312. The solution is then pumped to line 320 via line 313 and injected at a rate of 100 mls per minute through tee 315 into a seasoned Kodak 885 hardened fixer solution with a pH of about 4.8, flowing at a rate of 100 mls per minute in line 320. The resulting solution is then mixed within a tubular reactor 316. The solution is then returned to silver recovery unit 80 according to U.S. Pat. No. 5,437,792, which employs TMT as a silver precipitating agent and a flocculant to agglomerate the TMT-silver precipitate, as described above.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US05961939uspto-grants-1999_10