反应 #1810819

ord-01f965e2aae64f239953019f5b62f8c2

反应方程式

O=C(Cl)c1cc([N+](=O)[O-])ccc1N1CCOCC1
2-morpholin-4-yl-5-nitro-benzoyl chloride
N#Cc1ccc(C2=CCNCC2)cc1
4-(1,2,3,6-Tetrahydro-pyridin-4-yl)-benzonitrile
N#Cc1ccc(C2=CCN(C(=O)c3cc([N+](=O)[O-])ccc3N3CCOCC3)CC2)cc1
title compound
N#Cc1ccc(C2=CCN(C(=O)c3cc([N+](=O)[O-])ccc3N3CCOCC3)CC2)cc1
4-[1-(2-Morpholin-4-yl-5-nitro-benzoyl)-1,2,3,6-tetrahydro-pyridin-4-yl]benzonitrile

反应条件

详细条件
See reaction.notes.procedure_details.

后处理

  1. 1
    其他described for the synthesis of example 1

实验过程

According to the procedure described for the synthesis of example 1, the title compound has been synthesized from 2-morpholin-4-yl-5-nitro-benzoyl chloride and 4-(1,2,3,6-Tetrahydro-pyridin-4-yl)-benzonitrile (CAS: 460365-22-4). MS (m/e): 417.0 (M−H, 100%)

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US07485637B2uspto-grants-2009_02