反应 #1771990
ord-56238b79bf8e4876a8c816dff94dc2f6
反应方程式
tert-butyl N-tert-butoxycarbonyl-4,4-dimethylproline
→
4,4-Dimethylproline
反应条件
详细条件
See reaction.notes.procedure_details.
后处理
- 1浓缩The solution was concentrated
- 2其他dried under high vacuum
- 3其他taken to the next step without further purification
实验过程
A solution of tert-butyl N-tert-butoxycarbonyl-4,4-dimethylproline in dichloromethane (5 mL) and trifluoroacetic (5 mL) was stirred at room temperature for five hours. The solution was concentrated, dried under high vacuum and taken to the next step without further purification.