反应 #1702041
ord-2e75669cf5704c02b4b875fbbd2a1ae6
反应方程式
hydrochloric acid
sodium sulfate
zirconium oxychloride
→
zirconium sulfate
反应条件
温度
85°CELSIUS
详细条件
See reaction.notes.procedure_details.
后处理
- 1workup.ADDITIONwas added
- 2温度N, and the resulting product was maintained for 0.5 hour
实验过程
141 g of a 25% sodium sulfate solution was heated to 85° C. Then, 375 g of a zirconium oxychloride solution containing 16% of ZrO2 equivalent, previously heated to 85° C., was added thereto. Thereafter, hydrochloric acid was added so that the free acid concentration became 1.5; N, and the resulting product was maintained for 0.5 hour to form basic zirconium sulfate.