反应 #1687678

ord-29f7d2f806b94186be806bb94999d77d

反应方程式

C=Cc1ccc(O)cc1.C=Cc1ccccc1
p-hydroxystyrene styrene
C=COCC
vinylethyl ether
C=Cc1ccc(O)cc1.C=Cc1ccc(OCCOCC)cc1.C=Cc1ccccc1
p-1-ethoxyethoxystyrene p-hydroxystyrene styrene

反应条件

详细条件
See reaction.notes.procedure_details.

后处理

  1. 1
    其他obtained
  2. 2
    其他was carried out for reaction

实验过程

Using 15.0 g of poly(p-hydroxystyrene/styrene) obtained according to (2) above and 3.2 g of vinylethyl ether, the procedure of (3) of Preparation Example 1 was carried out for reaction and after-treatments to give 14.1 g of poly(p-1-ethoxyethoxystyrene/p-hydroxystyrene/styrene) as white powdery crystals. P-1-ethoxyethoxystyrene unit/p-hydroxystyrene unit/styrene unit molar ratio in the polymer≈32:60:8 (1H NMR). Mw≈18,000; Mw/Mn≈1.85 (GPC with polystyrene calibration).

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US05976759uspto-grants-1999_11