反应 #1687664

反应方程式

ethyl acrylate

methacrylamide

sodium

glycidyl methacrylate

4,4'-azobis-(4-cyanovaleric acid)

→

isobutyl methacrylate

溶剂

water

反应条件

后处理

1. 1
   workup.ADDITIONis added within 3 hours at 80° C
2. 2
   workup.ADDITIONare added simultaneously
3. 3
   其他obtains a coagulate-free dispersion with a solid content of 20%

实验过程

is added within 3 hours at 80° C. Thereafter a solution of 10 g of methacrylamide and 0.6 g of the sodium salt of 4,4'-azobis-(4-cyanovaleric acid) in 300 ml of water and a monomer mixture consisting of 50 g of ethyl acrylate and 45 g of glycidyl methacrylate are added simultaneously. After stirring for 60 minutes at 80° C. one obtains a coagulate-free dispersion with a solid content of 20%.

来源