反应 #1687635

反应方程式

fumarate

88

5-Methyl-2-(3-pyridyl)-thiazole

→

title compound

5-Methyl-2-(1-methyl-1,2,5,6-tetrahydro-3-pyridyl)-thiazole

反应条件

后处理

1. 1
   其他The crude free base obtained

实验过程

The title compound was prepared from 88 (2.2 g, 0.013 mol) by the procedure described in Example 49. The crude free base obtained, 89, was converted to the title fumarate, 90. Yield: 0.8 g (0.0032 mol, 25%). M.P. 159°-160° C. Anal. (C12H16N2O2S)C, H, N.

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