反应 #1619
ord-a3c93df638364213adea34d2adfb06d5
反应方程式
反应条件
详细条件
See reaction.notes.procedure_details.
后处理
- 1温度After cooling
- 2其他the solvent was evaporated
- 3其他the residue was dried
实验过程
A solution of (R)-3-(3,4-dimethoxyphenyl)-2-propylamine hydrochloride1 (500 mg, 2.15 mMol) in hydrogen bromide (48%, 5 ml) was stirred at 100° C. under an argon atmosphere for 20 hours. After cooling, the solvent was evaporated and the residue was dried giving the title compound.