反应 #1619

ord-a3c93df638364213adea34d2adfb06d5

反应条件

详细条件
See reaction.notes.procedure_details.

后处理

  1. 1
    温度After cooling
  2. 2
    其他the solvent was evaporated
  3. 3
    其他the residue was dried

实验过程

A solution of (R)-3-(3,4-dimethoxyphenyl)-2-propylamine hydrochloride1 (500 mg, 2.15 mMol) in hydrogen bromide (48%, 5 ml) was stirred at 100° C. under an argon atmosphere for 20 hours. After cooling, the solvent was evaporated and the residue was dried giving the title compound.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US05726165uspto-grants-1998_03