反应 #160987

ord-6ee8571305a044d68682dfacec6ed401

反应条件

详细条件
See reaction.notes.procedure_details.

后处理

  1. 1
    其他to afford an off-white powder

实验过程

The title compound was prepared in an analogous fashion to that described in Stage 9.3 using 5-bromo-6-chloronicotinic acid and 6-(trifluoromethylthio)pyridin-3-amine to afford an off-white powder. HPLC (Condition 4) tR=6.43 min, UPLC-MS (Condition 3) tR=1.15 min, m/z=411.9 [M−H]−.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US08829195B2uspto-grants-2014_09