反应 #1597021

ord-22bf736955ec46f7adb76f017b2e5be6

反应方程式

O=C(O)c1cc(Cl)ccc1O
5-chlorosalicylic acid
CC(C)(C)c1cccc(N)c1
3-tert-butylaniline
CC(C)(C)c1cccc(NC(=O)c2cc(Cl)ccc2O)c1
5-Chloro-N-(3-tert-butylphenyl)-2-hydroxybenzamide

反应条件

详细条件
See reaction.notes.procedure_details.

后处理

  1. 1
    其他This material was prepared

实验过程

This material was prepared according to the method of Example 1 using 5-chlorosalicylic acid and 3-tert-butylaniline with reagents and solvents employed in similar molar ratios. 1H NMR (500 MHz, DMSO-d6): δ 1.28 (s, 9H), 7.00 (d, 1H), 7.18 (m, 1H), 7.24 (m, 1H), 7.46 (dd, 1H), 7.56 (m, 1H), 7.68 (m, 1H), 7.95 (d, 1H), 10.38 (s, 1H), 11.90 (br s, 1H).

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US08211882B2uspto-grants-2012_07