反应 #1597021
ord-22bf736955ec46f7adb76f017b2e5be6
反应方程式
5-chlorosalicylic acid
3-tert-butylaniline
→
5-Chloro-N-(3-tert-butylphenyl)-2-hydroxybenzamide
反应条件
详细条件
See reaction.notes.procedure_details.
后处理
- 1其他This material was prepared
实验过程
This material was prepared according to the method of Example 1 using 5-chlorosalicylic acid and 3-tert-butylaniline with reagents and solvents employed in similar molar ratios. 1H NMR (500 MHz, DMSO-d6): δ 1.28 (s, 9H), 7.00 (d, 1H), 7.18 (m, 1H), 7.24 (m, 1H), 7.46 (dd, 1H), 7.56 (m, 1H), 7.68 (m, 1H), 7.95 (d, 1H), 10.38 (s, 1H), 11.90 (br s, 1H).