反应 #1597020
ord-b4584d49a54b4f1e87fd4be68b04716d
反应方程式
5-chlorosalicylic acid
3-aminobenzonitrile
→
5-Chloro-N-(3-cyanophenyl)-2-hydroxybenzamide
反应条件
详细条件
See reaction.notes.procedure_details.
后处理
- 1其他This material was prepared
实验过程
This material was prepared according to the method of Example 1 using 5-chlorosalicylic acid and 3-aminobenzonitrile, with reagents and solvents employed in similar molar ratios. 1HNMR (500 MHz, DMSO-d6): δ 3.72 (s, 3H), 6.74 (m, 1H), 7.05 (m, 1H), 7.45 (m, 1H), 7.58 (br m, 2H), 7.83 (m, 1H), 7.88 (m, 1H), 8.19 (br s, 1H), 10.59 (s, 1H).