反应 #1597019
ord-f35e4eb15faf4b21944933ddd46ed0c3
反应方程式
5-chlorosalicylic acid
m-anisidine
→
5-Chloro-2-hydroxy-N-(3-methoxyphenyl)benzamide
反应条件
详细条件
See reaction.notes.procedure_details.
后处理
- 1其他This material was prepared
实验过程
This material was prepared according to the method of Example 1 using 5-chlorosalicylic acid and m-anisidine, with reagents and solvents employed in similar molar ratios. 1HNMR (500 MHz, DMSO-d6): δ 3.72 (s, 3H), 6.74 (m, 1H), 7.09 (m, 1H), 7.26 (br m, 2H), 7.40 (br s, 1H), 7.47 (m, 1H), 7.88 (m, 1H), 10.34 (s, 1H).