反应 #1597016
ord-46521701bd6a429db9f8176d19f5783f
反应方程式
3,5-dichlorosalicylic acid
2-chloro-4-nitroaniline
→
3,5-dichloro-N-(2-chloro-4-nitrophenyl)-2 hydroxybenzamide
反应条件
详细条件
See reaction.notes.procedure_details.
后处理
- 1其他This material was prepared
实验过程
This material was prepared according to the method of Example 1 using 3,5-dichlorosalicylic acid and 2-chloro-4-nitroaniline, with reagents and solvents employed in similar molar ratios. 1HNMR (500 MHz, DMSO-d6): δ7.85 (m, 1H, H4), 7.98 (m, 1H, H5), 8.29 (m, 1H, H5′), 8.04 (m, 1H, H6), 8.44 (m, 1H, H3′), 8.55 (m, 1H, H6′).