反应 #1597012
ord-61e980915eb64b168dfa2c8be17ada49
反应方程式
5-aminosalicylic acid
3-(4-nitrophenyl)propyl bromide
→
5-[3-(4-nitrophenyl)-n-propyl]aminosalicylic acid
收率 50.4%
反应条件
详细条件
See reaction.notes.procedure_details.
后处理
- 1其他in Synthesis Example 1
实验过程
By following the similar procedure in Synthesis Example 1 by using 5-aminosalicylic acid (500 mg, 3.26 mmole) and 3-(4-nitrophenyl)propyl bromide (950 mg, 3.92 mmole), 520 mg (50% yield) of 5-[3-(4-nitrophenyl)-n-propyl]aminosalicylic acid was obtained as a pale yellow solid.: mp 229-231° C.