反应 #1597009
ord-37bdd83f36d94255ad1c3ea222904faa
反应方程式
5-aminosalicylic acid
pentafluorobenzyl bromide
→
5-(pentafluorobenzyl)aminosalicylic acid
收率 60.0%
反应条件
详细条件
See reaction.notes.procedure_details.
后处理
- 1其他in Synthesis Example 1
实验过程
By following the similar procedure in Synthesis Example 1 by using 5-aminosalicylic acid (500 mg, 3.26 mmole) and pentafluorobenzyl bromide (1.02 g, 3.92 mmole), 650 mg (60% yield) of 5-(pentafluorobenzyl)aminosalicylic acid was obtained as a white solid.: mp>190° C. (decompose).