反应 #1597002
ord-8c41e893f9694a3a8de50183059646fe
反应方程式
5-aminosalicylic acid
4-nitrophenethyl bromide
→
5-(4-nitrophenethyl)aminosalicylic acid
收率 90.3%
反应条件
详细条件
See reaction.notes.procedure_details.
后处理
- 1其他in Synthesis Example 1
实验过程
By following the similar procedure in Synthesis Example 1 by using 5-aminosalicylic acid (500 mg, 3.26 mmole) and 4-nitrophenethyl bromide (900 mg, 3.92 mmole), 890 mg (50% yield) of 5-(4-nitrophenethyl)aminosalicylic acid was obtained as a pale yellow solid.:mp 234-236° C.