反应 #1597001

反应方程式

5-aminosalicylic acid

4-nitrobenzoyl chloride

→

5-(4-nitrobenzoyl)aminosalicylic acid

收率 56.0%

反应条件

后处理

1. 1
   其他in Synthesis Example 1

实验过程

By following the similar procedure in Synthesis Example 1 by using 5-aminosalicylic acid (500 mg, 3.26 mmole) and 4-nitrobenzoyl chloride (700 mg, 3.77 mmole), 550 mg (56% yield) of 5-(4-nitrobenzoyl)aminosalicylic acid was obtained as a pale yellow solid.:mp 270-271° C.

来源