反应 #1596999
ord-1efe9fdd3f6846eb8bbff2f0e670935f
反应方程式
5-aminosalicylic acid
4-methoxybenzyl chloride
→
5-(4-methoxybenzyl)aminosalicylic acid
收率 50.0%
反应条件
详细条件
See reaction.notes.procedure_details.
后处理
- 1其他in Synthesis Example 1
实验过程
By following the similar procedure in Synthesis Example 1 by using 5-aminosalicylic acid (1.00 g, 6.53 mmole) and 4-methoxybenzyl chloride (1.23 g, 7.84 mmole), 890 mg (50% yield) of 5-(4-methoxybenzyl)aminosalicylic acid was obtained as a white solid.:mp 205-206° C.