反应 #158230

ord-6183f732df1949c2a490b2e4ae7362c5

反应条件

详细条件
See reaction.notes.procedure_details.

后处理

  1. 1
    其他was prepared
  2. 2
    其他for 10 hours

实验过程

A complex reducing agent was prepared by reacting sodium (0.034 g/4.86 mmol) and naphthalene (0.622/4.86 mmol) in 70 ml of tetrahydrofuran under Ar flow in a 250 ml 1-neck round flask for 10 hours.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US08822714B2uspto-grants-2014_09