反应 #1563887

ord-81815eb3c1d54bb1b2ab89da27304eb8

反应方程式

COc1ccccc1NC(=O)c1c(N)cccc1Sc1ccc([N+](=O)[O-])cc1
2-amino-N-(2-methoxyphenyl)-6-(4-nitrophenyl-thio)benzamide
Cl
HCl
COc1ccccc1NC(=O)c1c(N)cccc1Sc1ccc([N+](=O)[O-])cc1.Cl
2-amino-N-(2-methoxyphenyl)-6-(4-nitrophenyl-thio)benzamide hydrochloride
收率 94.2%

溶剂

反应条件

详细条件
See reaction.notes.procedure_details.

后处理

  1. 1
    过滤The reaction mixture was filtered
  2. 2
    其他to get White solid

实验过程

2-amino-N-(2-methoxyphenyl)-6-(4-nitrophenyl-thio)benzamide dissolved in EA, stirred at room temperature, while HCl is inlet till occurred to white solid. The reaction mixture was filtered to get White solid; 94.2% yield;

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US09402819B2uspto-grants-2016_08