反应 #1519114

反应方程式

3-aminocarbonylpropionate

hydroxylamine

→

N-hydroxy-3-aminocarbonylpropionamide

溶剂

dioxane

反应条件

后处理

1. 1
   其他purified by preparative reverse-phase (C18) HPLC

实验过程

3-aminocarbonylpropionate A-6 (0.1 mmol) is treated with dioxane (1 mL) and hydroxylamine (50% in water, 2 mL) for 1-3 days, and then purified by preparative reverse-phase (C18) HPLC to afford the desired N-hydroxy-3-aminocarbonylpropionamide (A-7).

来源