反应 #1509670

ord-d8218a4d94d2448f8c758e08153efec8

反应条件

详细条件
See reaction.notes.procedure_details.

后处理

  1. 1
    其他The crude reaction mixture
  2. 2
    其他was purified by reverse-phase preparative HPLC

实验过程

Following the procedure of Example 128b, (R)-2,6-dichloro-9-(tetrahydrofuran-3-yl)-9H-purine (b) was reacted with tyramine. The crude reaction mixture was purified by reverse-phase preparative HPLC. MS m/z 360.1 (M+1).

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US08927281B2uspto-grants-2015_01