反应 #1509667

反应方程式

2,4-dichloro-7H-pyrrolo[2,3-d]pyrimidine

2-iodopropane

→

title compound

2,4-dichloro-7-isopropyl-7H-pyrrolo[2,3-d]pyrimidine

反应条件

后处理

1. 1
   其他The crude residue was purified by silica gel chromatography (15 to 25% ethyl acetate in hexane eluant)

实验过程

Following the procedure of Example 15b, 2,4-dichloro-7H-pyrrolo[2,3-d]pyrimidine (0.5 g, 2.67 mmol) was reacted with 2-iodopropane. The crude residue was purified by silica gel chromatography (15 to 25% ethyl acetate in hexane eluant) to afford the title compound as a solid. MS m/z 230.2 (M+1).

来源