反应 #1470426

反应方程式

1-oxyl-2,2,6,6-tetramethyl-4-glycidyloxypiperidine

dimethylamine

→

title compound

收率 82.8%

1-Oxyl-2,2,6,6-tetramethyl-4-(2-hydroxy-3-dimethylaminopropoxy)piperidine

收率 82.8%

溶剂

water

反应条件

后处理

1. 1
   其他Water is then removed by vacuum distillation

实验过程

A mixture of 10.0 g (0.044 mol) of 1-oxyl-2,2,6,6-tetramethyl-4-glycidyloxypiperidine and 10 mL of 40% (ca. 0.091 mol) of dimethylamine (w/w) is dissolved in 100 mL of water and then stirred for 16 hours at ambient temperature. Water is then removed by vacuum distillation to leave 10 g of the title compound as a red oil.

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