反应 #1365727

反应方程式

1-methyl-pyrazolo[5,4-b]pyridine-5,6-dicarboxylic acid anhydride

3-chloro-2,6-diethylaniline

→

6-(3-Chloro-2,6-diethylphenyl)aminocarbonyl-l-methyl-pyrazolo[5,4-b]pyridine-5-carboxylic Acid

溶剂

tetrahydrofuran

反应条件

后处理

1. 1
   其他obtained above, a reaction

实验过程

In 100 ml of tetrahydrofuran was dissolved 8.0 g (39.4 mmol) of 1-methyl-pyrazolo[5,4-b]pyridine-5,6-dicarboxylic acid anhydride. After adding 7.23 g (39.4 mmol) of 3-chloro-2,6-diethylaniline to the solution obtained above, a reaction was carried out at ambient temperature for 12 hours.

来源