反应 #1365706

ord-8df9a23df07745eab43ba41bd6dfb9e9

反应方程式

COc1ccc(C=O)cc1
Anisaldehyde
CC(=O)O
acetic acid
O=S(=O)(O)O
sulfuric acid
COc1ccc(C=O)cc1.O=S(=O)(O)O
Anisaldehyde sulfuric acid

溶剂

反应条件

温度
100°CELSIUS
详细条件
See reaction.notes.procedure_details.

实验过程

Anisaldehyde (0.5 ml) is mixed with glacial acetic acid (10 ml), methanol (85 ml) and concentrated sulfuric acid (5 ml). This solution is sprayed onto the TLC plate, which is then heated at 100° C.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US06444233B1uspto-grants-2002_09