反应 #1350587

反应方程式

methyl 2-methyl-3-nitrobenzoate

→

Methyl 3-Amino-2-methylbenzoate

溶剂

methanol

反应条件

后处理

1. 1
   过滤the catalyst was filtered off
2. 2
   其他the solvent was removed

实验过程

210 g of methyl 2-methyl-3-nitrobenzoate (1.08 mol) were dissolved in 4 l of methanol, 21 g of Pd/C were added and the mixture was subsequently hydrogenated at ambient pressure. After the reaction had ended, the catalyst was filtered off and the solvent was removed. Yield: 178 g (quant.).

来源