反应 #1277970

ord-580b6dff96b84b95b49292334f0d0c27

反应方程式

CCCCOP(=O)(OCCCC)OCCCC
TBPA
NCCOCCOCC(=O)O
AEEA
CCCCOP(=O)(OCCCC)OCCCC.NCCOCCOCC(=O)O
TBPA AEEA

反应物

试剂

反应条件

详细条件
See reaction.notes.procedure_details.

实验过程

Reaction of TBPA with AEEA gives an TBPA/AEEA adduct. AEEA is sold in commerce by Dow Chemical. 43.6 mmol of TBPA was added to a round bottom flask with 51.00 grams of pure toluene. The mixture is heated to reflux after which 43.6 mmol of AEEA was added dropwise and the solution refluxed for one hour. The toluene is removed using a rotary evaporator to produce a yellow solid.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US08679990B2uspto-grants-2014_03