反应 #1277970
ord-580b6dff96b84b95b49292334f0d0c27
反应方程式
TBPA
AEEA
→
TBPA AEEA
反应条件
详细条件
See reaction.notes.procedure_details.
实验过程
Reaction of TBPA with AEEA gives an TBPA/AEEA adduct. AEEA is sold in commerce by Dow Chemical. 43.6 mmol of TBPA was added to a round bottom flask with 51.00 grams of pure toluene. The mixture is heated to reflux after which 43.6 mmol of AEEA was added dropwise and the solution refluxed for one hour. The toluene is removed using a rotary evaporator to produce a yellow solid.