反应 #1269886

反应方程式

(4-phenoxypyridin-3-yl)methanol

→

4-phenoxynicotinaldehyde

收率 106.5%

溶剂

THF

反应条件

后处理

1. 1
   过滤the reaction mixture was filtered (celite)
2. 2
   其他Removal of the solvent

实验过程

MnO2 (289 mg, 3.33 mmol) was added to a solution of (4-phenoxypyridin-3-yl)methanol (70 mg, 0.33 mmol) in THF (10 mL). After stiffing overnight the reaction mixture was filtered (celite). Removal of the solvent provided 4-phenoxynicotinaldehyde (70 mg, 95%). MS [M+H]+=200.1.

来源