反应 #1256745

反应方程式

Compound 40a

Isobutyldiisopropylsilane

diisopropylchlorosilane

→

Compound 44a

Cyclopropyldiisopropylsilane

溶剂

反应条件

实验过程

The procedure of synthesizing Compound 40a was repeated, except that diisopropylchlorosilane (4.10 mL, 96.0 mmol) and cyclopropylmagnesium bromide THF solution (1.0M, 100 mL) were employed, whereby the Compound 44a was obtained as a colorless liquid (boiling point; 35 mmHg, 86 to 89° C. fraction, 1.84 g, 50%).

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