反应 #1254

ord-4c3ca7fee7ca4cb68a75ae1c5be3919e

反应条件

详细条件
See reaction.notes.procedure_details.

后处理

  1. 1
    workup.DISTILLATIONafter excess thionyl chloride was distilled off

实验过程

4-Methylbenzoyl chloride was prepared in a conventional manner from 4-methylbenzoic acid and thionyl chloride and after excess thionyl chloride was distilled off, was used as the crude product in the side chain chlorination.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US05723613uspto-grants-1998_03